Facile and scalable synthesis of Ti5Si3 nanoparticles via solid-state route in an autoclave
نویسندگان
چکیده
منابع مشابه
Facile and scalable synthesis of Ti5Si3 nanoparticles in molten salts for metal-matrix nanocomposites.
We report a novel synthesis of Ti5Si3 nanoparticles (NPs) via the magnesio-reduction of TiO2 NPs and SiO2 in eutectic LiCl-KCl molten salts at 700 °C. The Ti5Si3 particle size (∼25 nm) is confined to the nanoscale due to the partial dissolution of Mg and silica in the molten salts and a subsequent heterogeneous reduction on the surface of the TiO2 NPs.
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ژورنال
عنوان ژورنال: Journal of Superhard Materials
سال: 2017
ISSN: 1063-4576,1934-9408
DOI: 10.3103/s106345761702006x